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BIOANALYTICAL METHOD

No.

Compound

Matrix

Method

LOQ (ng/mL)

Status

1

Acyclovir

Plasma

LCMS/MS

10

VALIDATED

2

Alprazolam

Plasma

LCMS/MS

0,2

VALIDATED

3

Amlodipine

Plasma

LCMS/MS

0,1

VALIDATED

4

Amoxicillin

Plasma

HPLC-UV

500

VALIDATED

5

Amoxicillin-Clavulanic Acid            

Plasma

LCMS/MS

300 - 125

VALIDATED

6

Aripriprazole

Plasma

LCMS/MS

0,5

VALIDATED

7

Atenolol

Plasma

HPLC-FL

12,5

VALIDATED

8

Atorvastatin

Plasma

LCMS/MS

0,1

VALIDATED

9

Azithromycin

Plasma

LCMS/MS

5

VALIDATED

10

Bisoprolol

Plasma

LCMS/MS

0,5

VALIDATED

11

Candesartan

Plasma

HPLC-FL

10

VALIDATED

12

Captopril

Plasma

HPLC-UV

10

VALIDATED

13

Carbamazepine

Plasma

HPLC-UV

10

VALIDATED

14

Carvedilol

Plasma

LCMS/MS

1

VALIDATED

15

Cefixime

Plasma

HPLC-UV

200

VALIDATED

16

Celecoxib

 Plasma

HPLC UV

10

VALIDATED

17

Cilostazol

Plasma

UPLC-UV

10

VALIDATED

18

Ciprofloxacin

Plasma

HPLC-UV

30

VALIDATED

19

Clarithromycin

Plasma

LCMS/MS

5

VALIDATED

20

Clopidrogel

Plasma

LCMS/MS

0,005

VALIDATED

21

Clozapine

 Plasma

LCMS/MS

2

VALIDATED

22

Co-Enzim Q10

 Plasma

HPLC UV

150

VALIDATED

23

Deferasirox

 Plasma

HPLC UV

100

VALIDATED

24

Duloxetin

Plasma

LCMS/MS

0.5

VALIDATED

25

Enalapril

Plasma

LCMS/MS

1

VALIDATED

26

Entecavir

Plasma

LCMS/MS

0.05

VALIDATED

27

Escitalopram

Plasma

LCMS/MS

0,2

VALIDATED

28

Evafirenz

Plasma

LCMS/MS

5

VALIDATED

29

Fenofibric Acid

 Plasma

UPLC-UV

100

VALIDATED

30

Fexofenadine

Plasma

LCMS/MS

5

VALIDATED

31

Fluconazole

Plasma

HPLC-UV

100

VALIDATED

32

Fluoxetine

Plasma

LCMS/MS

0.5

VALIDATED

33

Furosemide

Plasma

UPLC-UV

5

VALIDATED

34

Gabapentin

Plasma

LCMS/MS

50

VALIDATED

35

Gemfibrozil

Plasma

HPLC-UV

200

VALIDATED

36

Glibenclamide

 Plasma

LCMS/MS

1

VALIDATED

37

Gliclazide

Plasma

HPLC-UV

20

VALIDATED

38

Glimepiride

Plasma

LCMS/MS

1

VALIDATED

39

Glimepiride – Metformin

Plasma

LCMS/MS

1 – 20

VALIDATED

40

Gliquidone

Plasma

HPLC-UV

10

VALIDATED

41

Granisetron

Plasma

LCMS/MS

0.2

VALIDATED

42

Ibuprofen

Plasma

HPLC-UV

500

VALIDATED

43

Itraconazole

Plasma

LC-MS/MS

2

VALIDATED

44

Itraconazole + OH

Plasma

HPLC-FL

20

VALIDATED

45

Irbesartan

Plasma

HPLC-FL

30

VALIDATED

46

K-Diclofenac

Plasma

UPLC-UV

10

VALIDATED

47

Ketoconazole

Plasma

HPLC-FL

100

VALIDATED

48

Lamivudine

Plasma

HPLC-UV

25

VALIDATED

49

Lansoprazole

Plasma

LCMS/MS

5

VALIDATED

50

Levetiracetam

 Plasma

HPLC UV

200

VALIDATED

51

Levodopa

Plasma

LC-MS/MS

25

VALIDATED

52

Levofloxacin

Plasma

HPLC-FLD

20

VALIDATED

53

Levofloxacin

Cornea

HPLC-UV

40

VALIDATED

54

Lisinopril

Plasma

LC-MS/MS

1

VALIDATED

55

Losartan

Plasma

LCMS/MS

3

VALIDATED

56

Losartan Carboxy Acid

Plasma

LCMS/MS

3

VALIDATED

57

Meloxicam

Plasma

HPLC-UV

15

VALIDATED

58

Metformin

Plasma

HPLC-UV

25

VALIDATED

59

Metformin

Serum

HPLC UV

25

VALIDATED

60

Metoprolol Tartrate

Plasma

HPLC-FL

5

VALIDATED

61

Montelukast

 Plasma

HPLC-FL

5

VALIDATED

62

Moxifloxacin

Plasma

HPLC-UV

20

VALIDATED

63

Mycophenolic Acid

Plasma

UPLC-UV

100

VALIDATED

64

Na-Diclofenac

Plasma

UPLC-UV

5

VALIDATED

65

Nevirapine

Plasma

HPLC-UV

200

VALIDATED

66

Nimodipine

Plasma

LCMS/MS

0.5

VALIDATED

67

Norethindrone

Plasma

LCMS/MS

5

VALIDATED

68

Ofloxacin

Plasma

HPLC-UV

50

VALIDATED

69

Omeprazole

Plasma

LCMS/MS

5

VALIDATED

70

Ondansetron

Plasma

LCMS/MS

0,5

VALIDATED

71

Pantoprazole

Plasma

LCMS/MS

5

VALIDATED

72

Paracetamol

Plasma

HPLC-UV

100

VALIDATED

73

Phenytoin

Plasma

LCMS/MS

2

VALIDATED

74

Pioglitazone

Plasma

HPLC-UV

20

VALIDATED

75

Piracetam

Plasma

HPLC-UV

100

VALIDATED

76

Pregabalin

Plasma

LCMS/MS

100

VALIDATED

77

Pseudoephedrine

Plasma

HPLC-UV

20

VALIDATED

78

Pyridyl Acid

Plasma

LCMS/MS

3

VALIDATED

79

Ramipril

Plasma

LCMS/MS

0.1

VALIDATED

80

Ramiprilat

Plasma

LCMS/MS

0.5

VALIDATED

81

Rebamipide

Plasma

HPLC-UV

10

VALIDATED

82

Rifampicin

Plasma

UPLC-UV

50

VALIDATED

83

Risperidone

Plasma

LCMS/MS

0.25

VALIDATED

84

Rosuvastatin

 Plasma

LCMS/MS

0,1

VALIDATED

85

Sildenafil

Plasma

LCMS/MS

5

VALIDATED

86

Simvastatin

Plasma

LCMS/MS

0,2

VALIDATED

87

Spironolactone

Plasma

HPLC UV

20

VALIDATED

88

Telmisartan         

Plasma

HPLC FL

0.5

VALIDATED

89

Theophylline

Plasma

HPLC-UV

10

VALIDATED

90

Tramadol

Plasma

HPLC-UV

10

VALIDATED

91

Trimetazidine

Plasma

GC/MS

5

VALIDATED

92

Valsartan            

Plasma

HPLC FL

20

VALIDATED

93

Voriconazole

Plasma

HPLC-UV

50

VALIDATED

94

Valproic acid

Plasma

LCMS/MS

500

VALIDATED

95

Zopiclone

Plasma

LCMS/MS

1

VALIDATED

May 2017

 

METHOD UNDER DEVELOPMENT

No.

Compound

Matrix

Method

LOQ (ng/mL)

Status

1

Ethynil Estradiol

Plasma

LCMS/MS

0.001

IDENTIFIED

2

Cyproterone Acetate

Plasma

LCMS/MS

0.4

IDENTIFIED

3

Ticagrelor

Plasma

LC-MS/MS

10

IDENTIFIED

4

Pyrazinamid

Plasma

UPLC-UV

50

IDENTIFIED

5

Warfarin

Plasma

UPLC-UV

10

IDENTIFIED

6

6-Thioguanine

Serum

LC-MS/MS

10

IDENTIFIED

7

6-Methyl Mercaptopurine

Serum

LC-MS/MS

10

IDENTIFIED

8

Levonorgestrel

Plasma

LC-MS/MS

0.1

IDENTIFIED

9

Risedronate Sodium

Plasma

LC-MS/MS

0.5

IDENTIFIED

May 2017